{"id":26174,"date":"2022-03-21T14:05:18","date_gmt":"2022-03-21T06:05:18","guid":{"rendered":"https:\/\/www.accscicn.com\/?p=26174"},"modified":"2022-10-20T17:48:09","modified_gmt":"2022-10-20T09:48:09","slug":"app_high_frequency_analyzers","status":"publish","type":"post","link":"https:\/\/www.accscicn.com\/en\/insight\/application\/app_high_frequency_analyzers\/","title":{"rendered":"4990EDMS-120K high frequency impedance analyzer for fluoride conductivity measurement case"},"content":{"rendered":"<div data-elementor-type=\"wp-post\" data-elementor-id=\"26174\" class=\"elementor elementor-26174\" data-elementor-post-type=\"post\">\n\t\t\t\t\t\t<section class=\"elementor-section elementor-top-section elementor-element elementor-element-7f189a37 elementor-section-full_width elementor-section-stretched elementor-section-height-default elementor-section-height-default\" data-id=\"7f189a37\" data-element_type=\"section\" data-settings=\"{&quot;stretch_section&quot;:&quot;section-stretched&quot;,&quot;background_background&quot;:&quot;classic&quot;}\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-100 elementor-top-column elementor-element elementor-element-4278d49b\" data-id=\"4278d49b\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<section class=\"elementor-section elementor-inner-section elementor-element elementor-element-22a6c415 elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"22a6c415\" data-element_type=\"section\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-a65d91f\" data-id=\"a65d91f\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-a9acd94 elementor-widget elementor-widget-heading\" data-id=\"a9acd94\" data-element_type=\"widget\" data-widget_type=\"heading.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t<style>\/*! elementor - v3.21.0 - 20-05-2024 *\/\n.elementor-heading-title{padding:0;margin:0;line-height:1}.elementor-widget-heading .elementor-heading-title[class*=elementor-size-]>a{color:inherit;font-size:inherit;line-height:inherit}.elementor-widget-heading .elementor-heading-title.elementor-size-small{font-size:15px}.elementor-widget-heading .elementor-heading-title.elementor-size-medium{font-size:19px}.elementor-widget-heading .elementor-heading-title.elementor-size-large{font-size:29px}.elementor-widget-heading .elementor-heading-title.elementor-size-xl{font-size:39px}.elementor-widget-heading .elementor-heading-title.elementor-size-xxl{font-size:59px}<\/style><h3 class=\"elementor-heading-title elementor-size-default\">Influence of microstructure on the electrical conductivity of Tysonite-type fluorine-ion conductors<\/h3>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-189d0fb7 elementor-widget elementor-widget-text-editor\" data-id=\"189d0fb7\" data-element_type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t<style>\/*! elementor - v3.21.0 - 20-05-2024 *\/\n.elementor-widget-text-editor.elementor-drop-cap-view-stacked .elementor-drop-cap{background-color:#69727d;color:#fff}.elementor-widget-text-editor.elementor-drop-cap-view-framed .elementor-drop-cap{color:#69727d;border:3px solid;background-color:transparent}.elementor-widget-text-editor:not(.elementor-drop-cap-view-default) .elementor-drop-cap{margin-top:8px}.elementor-widget-text-editor:not(.elementor-drop-cap-view-default) .elementor-drop-cap-letter{width:1em;height:1em}.elementor-widget-text-editor .elementor-drop-cap{float:left;text-align:center;line-height:1;font-size:50px}.elementor-widget-text-editor .elementor-drop-cap-letter{display:inline-block}<\/style>\t\t\t\t<p>In the present study, Tysonite-type fluorine ionic conductors La0.93Ba0.07F2.93 dense sintered polycrystalline briquettes (relative density: &gt;95%) with different grain sizes were prepared by discharge plasma sintering and their electrical conductivities were investigated. An evaluation was carried out to understand the effect of microstructure on ionic conductivity. The electrical conductivity of the prepared briquettes increased when the sintering temperature was raised to 1273 K and exhibited the highest value, e.g. 7.1 \u00d7 10-5Scm-1 at 300 K, which is much higher than the reported value for sintered bodies of the same material. This is due to the fact that the application of discharge plasma sintering technology enables us to achieve high densification of the sintered body and the increase in sintering temperature promotes grain growth, leading to a decrease in grain boundary resistance. When the density of the polycrystalline composite is high enough, the inhibitory effect of grain boundaries on ionic conduction is not significant. On the other hand, when the sintering temperature is higher than 1273 K, small pores are formed along the grain boundaries, and the electrical conductivity decreases as the sintering temperature increases. This decrease in conductivity can be explained as an increase in grain boundary resistance due to hole formation resulting from high temperature sintering. This work shows that for sintered polycrystalline (La,Ba)F3-based fluoride ion conductors, there is an optimal preparation condition to achieve the best microstructure, i.e., high density, large grain size, and clean grain boundaries for high fluoride ion conduction.<img fetchpriority=\"high\" decoding=\"async\" class=\"alignnone size-full wp-image-26177\" src=\"https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/03\/\u5fae\u4fe1\u56fe\u7247_20220321134235.png\" alt=\"\" width=\"1547\" height=\"1259\" srcset=\"https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/03\/\u5fae\u4fe1\u56fe\u7247_20220321134235.png 1547w, https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/03\/\u5fae\u4fe1\u56fe\u7247_20220321134235-300x244.png 300w, https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/03\/\u5fae\u4fe1\u56fe\u7247_20220321134235-1024x833.png 1024w, https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/03\/\u5fae\u4fe1\u56fe\u7247_20220321134235-768x625.png 768w, https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/03\/\u5fae\u4fe1\u56fe\u7247_20220321134235-1536x1250.png 1536w\" sizes=\"(max-width: 1547px) 100vw, 1547px\" \/><\/p><p>In this thesis, observations were made using a high-frequency analyzer, 4990EDMS-120K LN-Z2-HF, Toyo Co., Japan, on LBF93 blocks sintered at 1073, 1273, 1373, and 1473 K, respectively, at room temperature.<br \/>See the original article for details.<\/p><p>Source:<\/p><p><span style=\"text-decoration: underline;\"><a href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S016727381930356X\">Influence of microstructures on conductivity in Tysonite-type fluoride ion conductors<\/a><\/span><br \/>Author: K. Motohashi,T. Nakamura,Y. Kimura,Y. Uchimoto,K. Amezawa<br \/>Publication: Solid State Ionics<br \/>Publisher: Elsevier<br \/>Date: 1 October 2019<br \/>https:\/\/doi.org\/10.1016\/j.ssi.2019.05.023<\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-fa6bfc0\" data-id=\"fa6bfc0\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-5bff8d6c elementor-widget-divider--view-line elementor-widget elementor-widget-divider\" data-id=\"5bff8d6c\" data-element_type=\"widget\" data-widget_type=\"divider.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t<style>\/*! elementor - v3.21.0 - 20-05-2024 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href=\"https:\/\/www.accscicn.com\/en\/product\/impedance-analyzer\/\" aria-label=\"Read more about 4990EDMS-120K\u9ad8\u9891\u963b\u6297\u5206\u6790\u4eea\" tabindex=\"-1\" >\n\t\t\tRead More \"\t\t<\/a>\n\n\t\t\t\t<\/div>\n\t\t\t\t<\/article>\n\t\t\t\t<\/div>\n\t\t\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<\/div>","protected":false},"excerpt":{"rendered":"<p>\u5fae\u7ed3\u6784\u5bf9 Tysonite \u578b\u6c1f\u79bb\u5b50\u5bfc\u4f53 [&hellip;]<\/p>","protected":false},"author":1,"featured_media":26177,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","theme-transparent-header-meta":"","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"default","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center 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