{"id":26224,"date":"2022-04-22T21:44:12","date_gmt":"2022-04-22T13:44:12","guid":{"rendered":"https:\/\/www.accscicn.com\/?p=26224"},"modified":"2022-10-20T17:44:59","modified_gmt":"2022-10-20T09:44:59","slug":"app_fce10_003","status":"publish","type":"post","link":"https:\/\/www.accscicn.com\/es\/vision\/aplicacion\/app_fce10_003\/","title":{"rendered":"Crecimiento hidrotermal de l\u00e1minas delgadas ferroel\u00e9ctricas de (Bi1\/2K1\/2)TiO3 con orientaci\u00f3n en el eje c sobre sustratos met\u00e1licos"},"content":{"rendered":"<div data-elementor-type=\"wp-post\" data-elementor-id=\"26224\" class=\"elementor elementor-26224\" data-elementor-post-type=\"post\">\n\t\t\t\t\t\t<section class=\"elementor-section elementor-top-section elementor-element elementor-element-6e26442c elementor-section-full_width elementor-section-stretched elementor-section-height-default elementor-section-height-default\" data-id=\"6e26442c\" data-element_type=\"section\" data-settings=\"{&quot;stretch_section&quot;:&quot;section-stretched&quot;,&quot;background_background&quot;:&quot;classic&quot;}\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-100 elementor-top-column elementor-element elementor-element-5e77bc98\" data-id=\"5e77bc98\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<section class=\"elementor-section elementor-inner-section elementor-element elementor-element-2bbcaf76 elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"2bbcaf76\" data-element_type=\"section\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-e14a052\" data-id=\"e14a052\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-6b79fc6a elementor-widget elementor-widget-heading\" data-id=\"6b79fc6a\" data-element_type=\"widget\" data-widget_type=\"heading.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t<style>\/*! elementor - v3.21.0 - 20-05-2024 *\/\n.elementor-heading-title{padding:0;margin:0;line-height:1}.elementor-widget-heading .elementor-heading-title[class*=elementor-size-]>a{color:inherit;font-size:inherit;line-height:inherit}.elementor-widget-heading .elementor-heading-title.elementor-size-small{font-size:15px}.elementor-widget-heading .elementor-heading-title.elementor-size-medium{font-size:19px}.elementor-widget-heading .elementor-heading-title.elementor-size-large{font-size:29px}.elementor-widget-heading .elementor-heading-title.elementor-size-xl{font-size:39px}.elementor-widget-heading .elementor-heading-title.elementor-size-xxl{font-size:59px}<\/style><h3 class=\"elementor-heading-title elementor-size-default\">Crecimiento hidrotermal de l\u00e1minas delgadas ferroel\u00e9ctricas de (Bi1\/2K1\/2)TiO3 con orientaci\u00f3n en el eje c sobre sustratos met\u00e1licos<\/h3>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-484e15a4 elementor-widget elementor-widget-text-editor\" data-id=\"484e15a4\" data-element_type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t<style>\/*! elementor - v3.21.0 - 20-05-2024 *\/\n.elementor-widget-text-editor.elementor-drop-cap-view-stacked .elementor-drop-cap{background-color:#69727d;color:#fff}.elementor-widget-text-editor.elementor-drop-cap-view-framed .elementor-drop-cap{color:#69727d;border:3px solid;background-color:transparent}.elementor-widget-text-editor:not(.elementor-drop-cap-view-default) .elementor-drop-cap{margin-top:8px}.elementor-widget-text-editor:not(.elementor-drop-cap-view-default) .elementor-drop-cap-letter{width:1em;height:1em}.elementor-widget-text-editor .elementor-drop-cap{float:left;text-align:center;line-height:1;font-size:50px}.elementor-widget-text-editor .elementor-drop-cap-letter{display:inline-block}<\/style>\t\t\t\t<h4>Presentaci\u00f3n<\/h4><p>Recientemente, con el r\u00e1pido desarrollo de la tecnolog\u00eda, las l\u00e1minas delgadas ferroel\u00e9ctricas se utilizan ampliamente en diversos dispositivos electr\u00f3nicos modernos, como memorias de acceso aleatorio, interruptores \u00f3pticos, aceler\u00f3metros, etc. . Y, con el r\u00e1pido desarrollo de las redes de sensores inal\u00e1mbricos, el uso de captadores de energ\u00eda piezoel\u00e9ctricos con l\u00e1minas delgadas ferroel\u00e9ctricas como fuente de energ\u00eda para nodos de sensores inal\u00e1mbricos ha atra\u00eddo cada vez m\u00e1s atenci\u00f3n. Los captadores de energ\u00eda piezoel\u00e9ctricos convierten la energ\u00eda mec\u00e1nica de las vibraciones ambientales en energ\u00eda el\u00e9ctrica mediante el efecto piezoel\u00e9ctrico directo de las pel\u00edculas ferroel\u00e9ctricas. Dado que la mayor\u00eda de las vibraciones ambientales tienen una frecuencia baja, de unos 10-200 Hz, es necesario ajustar el cosechador resonante a una frecuencia tan baja manteniendo al mismo tiempo el tama\u00f1o del dispositivo en un nivel reducido. Por lo tanto, las pel\u00edculas ferroel\u00e9ctricas formadas sobre sustratos met\u00e1licos con bajo m\u00f3dulo de Young son ideales para aplicaciones de captaci\u00f3n de energ\u00eda.<\/p><p>Los metales b\u00e1sicos de bajo coste, como el n\u00edquel, el aluminio y el cobre, se oxidan f\u00e1cilmente a altas temperaturas en el aire. Adem\u00e1s, las propiedades piezoel\u00e9ctricas y de captaci\u00f3n de energ\u00eda de las l\u00e1minas finas ferroel\u00e9ctricas dependen en gran medida de la orientaci\u00f3n y el grosor del cristal. Por lo tanto, es especialmente importante desarrollar un proceso de crecimiento de pel\u00edculas ferroel\u00e9ctricas a baja temperatura que permita controlar la orientaci\u00f3n del cristal y el grosor de la pel\u00edcula. Los m\u00e9todos hidrotermales son una t\u00e9cnica de s\u00edntesis a baja temperatura para obtener materiales cristalinos a partir de soluciones acuosas y se han descrito para la deposici\u00f3n de \u00f3xidos ferroel\u00e9ctricos como Pb(Zr,Ti)O3 (PZT), BaTiO3, BiFeO3 (BF) y (K,Na)NbO3 (KNN), para pel\u00edculas delgadas ferroel\u00e9ctricas cultivadas hidrotermalmente sobre sustratos met\u00e1licos, (Morita et al.), a una temperatura baja de 160 \u00b0C. Se fabricaron pel\u00edculas de PZT sobre sustratos de titanio mediante reacci\u00f3n hidrotermal a 160 \u00b0C. Se ha reportado que el m\u00e9todo hidrotermal es capaz de depositar pel\u00edculas gruesas de KNN orientado de hasta 27 \u03bcm de espesor sobre sustratos de aleaciones basadas en n\u00edquel [14-16]. Estos trabajos previos demuestran que los m\u00e9todos hidrot\u00e9rmicos son una t\u00e9cnica potente para fabricar pel\u00edculas delgadas ferroel\u00e9ctricas sobre sustratos met\u00e1licos de bajo coste.<\/p><p>Los ferroel\u00e9ctricos basados en PZT se consideran los materiales m\u00e1s prometedores para aplicaciones de captaci\u00f3n de energ\u00eda debido a sus excelentes propiedades piezoel\u00e9ctricas. Sin embargo, la b\u00fasqueda de materiales ferroel\u00e9ctricos alternativos sin plomo es cada vez m\u00e1s importante debido a la gran preocupaci\u00f3n que suscita el impacto medioambiental negativo del plomo. Se ha informado de que los \u00f3xidos de calcogenuro que contienen bismuto, como el BF, presentan excelentes propiedades ferroel\u00e9ctricas debido a la configuraci\u00f3n electr\u00f3nica del Bi3+ con 6s 2 electrones de par solitario, que es la misma que la del Pb2+. Recientemente, nuestro grupo ha desarrollado un proceso de s\u00edntesis hidrotermal de part\u00edculas finas y cer\u00e1micas a granel de titanato de bismuto pot\u00e1sico (Bi1\/2K1\/2).<\/p><p>El TiO3 (BKT) es un cuerpo ferroel\u00e9ctrico con estructura de calcogenuro tetragonal. Estudios posteriores de cer\u00e1micas BKT a granel han demostrado que el BKT tiene buenas propiedades piezoel\u00e9ctricas para aplicaciones de captaci\u00f3n de energ\u00eda, como constantes piezoel\u00e9ctricas relativamente altas (d33 ~ 95 pC\/N), altas temperaturas de despolarizaci\u00f3n (Td ~ 300 \u00b0C) y constantes diel\u00e9ctricas bajas (\u03b5r ~ 600). Sin embargo, se ha informado muy poco sobre la preparaci\u00f3n y deposici\u00f3n de pel\u00edculas de BKT. Hasta la fecha, no se ha desarrollado ninguna tecnolog\u00eda para pel\u00edculas BKT sobre sustratos met\u00e1licos.<\/p><p>En este informe aplicamos el m\u00e9todo hidrot\u00e9rmico a la fabricaci\u00f3n de pel\u00edculas de BKT sobre sustratos met\u00e1licos de aleaci\u00f3n basados en n\u00edquel. LaNiO3 (LN), un \u00f3xido calcogenuro conductor, se deposit\u00f3 como capa tamp\u00f3n sobre el sustrato mediante recubrimiento sol-gel para promover la nucleaci\u00f3n heterog\u00e9nea de BKT. Demostramos que las pel\u00edculas de BKT con una orientaci\u00f3n preferente en el eje c pueden crecer sobre sustratos tamp\u00f3n de LN mediante reacciones hidrotermales a temperaturas tan bajas como 150 \u00b0C. En esta aproximaci\u00f3n, la estructura superficial y el espesor de las pel\u00edculas de BKT pueden controlarse mediante el n\u00famero de ciclos de deposici\u00f3n de LN y BKT, respectivamente. Tambi\u00e9n se presentan las propiedades diel\u00e9ctricas y ferroel\u00e9ctricas de las pel\u00edculas de BKT resultantes.<\/p><p>\u00a0<\/p><h4>Aplicaciones<\/h4><p>En este art\u00edculo nos centramos en la idoneidad de las l\u00e1minas delgadas ferroel\u00e9ctricas fabricadas sobre sustratos met\u00e1licos para su uso en captadores de energ\u00eda por vibraci\u00f3n piezoel\u00e9ctrica. En este informe, demostramos que las pel\u00edculas densas ferroel\u00e9ctricas sin plomo (Bi1\/2K1\/2)TiO3 (BKT) con una orientaci\u00f3n preferente en el eje c pueden crecer sobre sustratos de aleaci\u00f3n con base de n\u00edquel utilizando un m\u00e9todo de s\u00edntesis hidrotermal. Se form\u00f3 una capa tamp\u00f3n de LaNiO3 (LN) sobre el sustrato mediante recubrimiento sol-gel y, a continuaci\u00f3n, se cultiv\u00f3 BKT mediante reacci\u00f3n hidrot\u00e9rmica a una temperatura baja de 150 \u00b0C. Se observ\u00f3 que la estructura superficial y el espesor de las pel\u00edculas finales de BKT dependen en gran medida del n\u00famero de ciclos de deposici\u00f3n de LN y BKT, respectivamente. Como resultado, se obtuvieron pel\u00edculas de BKT altamente orientadas en el eje c con superficies lisas y espesores de hasta 830 nm. Aunque las pel\u00edculas de BKT depositadas conten\u00edan grupos hidroxilo en su red, se eliminaron eficazmente mediante un proceso de recocido posterior a 650\u00b0C en aire, y la respuesta de polarizaci\u00f3n de las pel\u00edculas de BKT recocidas demostr\u00f3 una transici\u00f3n de electr\u00f3lisis de hierro en las pel\u00edculas.<\/p><h4><img fetchpriority=\"high\" decoding=\"async\" class=\"alignnone size-full wp-image-26227\" src=\"https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/04\/image-2.png\" alt=\"\" width=\"1106\" height=\"354\" srcset=\"https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/04\/image-2.png 1106w, https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/04\/image-2-300x96.png 300w, https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/04\/image-2-1024x328.png 1024w, https:\/\/www.accscicn.com\/wp-content\/uploads\/2022\/04\/image-2-768x246.png 768w\" sizes=\"(max-width: 1106px) 100vw, 1106px\" \/><\/h4><p>La imagen 10 muestra la superficie y la estructura transversal de la pel\u00edcula observadas mediante microscop\u00eda electr\u00f3nica de barrido por emisi\u00f3n de campo (FE-SEM) utilizando un microscopio FEI Sirion a una tensi\u00f3n de aceleraci\u00f3n de 5 kV. El tama\u00f1o medio de grano se determin\u00f3 midiendo las longitudes de los bordes de los 30 granos c\u00fabicos encontrados en las im\u00e1genes FE-SEM de la superficie de la pel\u00edcula. La determinaci\u00f3n de fase de las pel\u00edculas se llev\u00f3 a cabo mediante an\u00e1lisis de difracci\u00f3n de rayos X (DRX) utilizando un difract\u00f3metro Bruker AXS D8-ADVANCE con geometr\u00eda 2\u03b8\/\u03b8 de radiaci\u00f3n Cu K\u03b1. Para la caracterizaci\u00f3n el\u00e9ctrica, las pel\u00edculas depositadas fueron post recocidas en aire a 650\u00b0C durante 10 minutos para eliminar los grupos hidroxilo reticulares contenidos en las pel\u00edculas. A continuaci\u00f3n, se pulveriz\u00f3 un electrodo circular de oro de 1 mm de di\u00e1metro sobre la muestra de pel\u00edcula como electrodo superior y un sustrato de Inconel como electrodo inferior. Utilizando un medidor LCR (ZM2371, NF Inc.). Las curvas de polarizaci\u00f3n (P) frente al campo el\u00e9ctrico (E) y de densidad de corriente (J) frente a E se midieron a temperatura ambiente aplicando una onda de tensi\u00f3n delta a una frecuencia de 200 Hz utilizando un sistema de ensayo ferroel\u00e9ctrico (FCE10-B, TOYO Corp.).<\/p><p>\u00a0<\/p><h4><strong>Fuente<\/strong><\/h4><p>Autores: Masayoshi Yamamoto1, Ryotaro Sakurai, Manabu Hagiwara, Shinobu Fujihara<\/p><p>Instituci\u00f3n: Departamento de Qu\u00edmica Aplicada, Facultad de Ciencia y Tecnolog\u00eda, Universidad de Keio, 3-14-1Hiyoshi, Kohoku-ku, Yokohama 223-8522, Jap\u00f3n.<\/p><p>Publicado: Recibido el 15 de abril de 2020; Recibido en forma revisada el 17 de agosto de 2020; Aceptado el 8 de septiembre de 2020.<\/p><p>Palabras clave: ferroel\u00e9ctricos, crecimiento de l\u00e1minas delgadas, m\u00e9todo hidrot\u00e9rmico, sustratos met\u00e1licos, s\u00edntesis a baja temperatura<\/p><p>Revista: Thin SolidFilms<\/p><p>Sitio web fuente del art\u00edculo.<a href=\"https:\/\/sciencedirect.53yu.com\/science\/article\/abs\/pii\/S0040609020305514\" target=\"_blank\" rel=\"noopener\">Crecimiento hidrotermal de pel\u00edculas ferroel\u00e9ctricas (Bi1\/2K1\/2)TiO3 orientadas en el eje c sobre sustratos met\u00e1licos<\/a><\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-7332bd5\" data-id=\"7332bd5\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t<div class=\"elementor-element elementor-element-6c4adfa elementor-widget-divider--view-line elementor-widget elementor-widget-divider\" data-id=\"6c4adfa\" data-element_type=\"widget\" data-widget_type=\"divider.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t<style>\/*! elementor - v3.21.0 - 20-05-2024 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class=\"elementor-widget-container\">\n\t\t\t<h2 class=\"elementor-heading-title elementor-size-default\">Productos relacionados<\/h2>\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t<div class=\"elementor-element elementor-element-44f76f4c elementor-grid-1 elementor-grid-tablet-2 elementor-grid-mobile-1 elementor-posts--thumbnail-top elementor-widget elementor-widget-posts\" data-id=\"44f76f4c\" data-element_type=\"widget\" data-settings=\"{&quot;classic_columns&quot;:&quot;1&quot;,&quot;classic_columns_tablet&quot;:&quot;2&quot;,&quot;classic_columns_mobile&quot;:&quot;1&quot;,&quot;classic_row_gap&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:35,&quot;sizes&quot;:[]},&quot;classic_row_gap_tablet&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:&quot;&quot;,&quot;sizes&quot;:[]},&quot;classic_row_gap_mobile&quot;:{&quot;unit&quot;:&quot;px&quot;,&quot;size&quot;:&quot;&quot;,&quot;sizes&quot;:[]}}\" data-widget_type=\"posts.classic\">\n\t\t\t\t<div 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aria-label=\"M\u00e1s informaci\u00f3n sobre FCE10\u94c1\u7535\u6750\u6599\u6d4b\u8bd5\u8bbe\u5907\" tabindex=\"-1\" >\n\t\t\tLeer M\u00e1s \"\t\t<\/a>\n\n\t\t\t\t<\/div>\n\t\t\t\t<\/article>\n\t\t\t\t<\/div>\n\t\t\n\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<section class=\"elementor-section elementor-inner-section elementor-element elementor-element-28b48293 elementor-section-boxed elementor-section-height-default elementor-section-height-default\" data-id=\"28b48293\" data-element_type=\"section\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-default\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column elementor-element elementor-element-592f4f6\" data-id=\"592f4f6\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap\">\n\t\t\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t<div class=\"elementor-column elementor-col-50 elementor-inner-column 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